Analytical Sciences

Abstract − Analytical Sciences, 19(2), 337 (2003).

Crystal Structure of Tetracarbonyl(2,2'-dipyridylamine)tungsten
Fenghui LIU, Wanzhi CHEN,  and Xiaozeng YOU
State Key Laboratory of Coordination Chemistry, Coordination Chemistry Institute, Department of Chemistry, Nanjing University, Nanjing 210093, P. R. China
Tetracarbonyl(2,2'-dipyridylamine)tungsten was prepared from W(CO)6 and 2,2'-dipyridylamine in toluene. The structure was determined by an X-ray diffraction analysis. Crystal data: triclinic; space group, P-1 (No.2); a = 8.454(1)Å, b = 13.369(2)Å, c = 6.9452(9) Å, alpha= 85.88(1)°, beta= 68.28(1)°, gamma= 80.93(1)°, V = 720.0(1)Å3; Z = 2.